sample preparation
Learn how to test your sample material before comminution – including tips on pretreatment, consideration of moisture, agglomeration, and determining the ideal sample size.
Solids and bulk materials must be ground if their grain size is too coarse for processes such as analysis, mixing, or further processing. Methods such as spectroscopy and chromatography are used for quality assurance. Since grain size often influences product properties (e.g., extraction, filtration, absorption), ground material is also essential in the laboratory for product development and production processes.
It is often required that materials be ground to a “powder-fine” state – a term that, however, has no clear definition, since bulk materials such as washing powder, coffee powder and baking powder vary greatly in grain size and distribution.
Likewise, laboratory samples are required to be ground "as finely as possible," which, however, requires high energy consumption, a long time, and thus increased costs. The motto is therefore: not finer than possible, but only as fine as necessary.
In addition, the sample material must have the required fineness for the respective analysis method, which is usually between 20 µm and 2 mm.
For optimal comminution, the device's mechanism must be tailored to the material's fracture behavior. Therefore, the material properties—such as density, hardness, consistency, residual moisture, fat content, temperature sensitivity, agglomeration behavior, and surface reactions—must be carefully examined before processing. Subsequent analysis must also be considered.
Further detailed information can be found here:
Solids and bulk materials must be ground if their original grain size is too coarse for analytical procedures, mixing processes, or further processing. Comminution is particularly essential in laboratories, as grain size directly influences product properties such as extraction, filtration, or absorption.
Solids and bulk materials must be ground if their original grain size is too coarse for analytical procedures, mixing processes, or further processing. Comminution is particularly essential in laboratories, as grain size directly influences product properties such as extraction, filtration, or absorption.
The required fineness depends on the chosen analytical method. Typically, the requirements are between 20 µm and 2 mm. Overgrinding should be avoided, as it consumes unnecessary energy and time.
For effective shredding, the material properties Factors such as density, hardness, moisture content, fat content, consistency, temperature behavior, and agglomeration must be taken into account. The selected analytical method also plays an important role in selecting the appropriate comminution process.
The selection of the appropriate grinding material (e.g., steel, ceramic, tungsten carbide) significantly influences the service life and performance of the mill. Depending on the analysis objective, possible material contamination due to abrasion should also be considered.